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Quality standard of traditional Chinese medicines: comparison between European Pharmacopoeia and Chinese Pharmacopoeia and recent advances

Samples from cohort 1 and cohort 7 were tested as representative samples from the SAD and MAD cohorts, respectively

see NMR-STAR file Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 1: 1D 1H, 0.5 mM Sample: 0.5mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 2: 1D 1H, 2.0 mM Sample: 2.0mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 3: 1D 1H Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 4: 2D [1H,1H]-TOCSY Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 5: 1D 13C Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 6: 1D DEPT90 Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 7: 1D DEPT135 Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 8: 2D [1H,13C]-HSQC Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 9: 2D [1H,13C]-HMBC Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 10: 2D [1H,1H]-COSY Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 500MHz 11: 2D [1H,13C]-HSQC SW small Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz